A novel analytical method has been established for on-line simultaneous determination of fluorene and acenaphthene by polarization synchronous fluorometry(PSF)hyphenated with HPLC.

• 本文以高效液相色谱(HPLC)作为分离手段,以偏振同步荧光法为检测手段,实现了环境样品中芴、苊的在线同时测定。