Synthesis of carbyne by oxidation polycondensation of dicopper acetylide with Cu~(1+) and Cu~(2+) coordination as catalysis was studied by FTIR, DSC and SEM.

• 用FTIR、DSC及SEM对Cu+和Cu2+的催化氧化乙炔化物缩聚合成线型碳进行了研究,结果表明:Cu2+发挥了关键的作用;