The high performance liquid chromatographic (HPLC) method with post column derivatization and fluorometric detection was developed for determination of gentamicin (one of the aminoglycosides) in milk.

• 摘要建立了庆大霉素（氨基苷类抗生素）在牛奶中残留量柱后衍生高效液相色谱检测法。