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- Preparation and Evaluation of Mixed-Mode Silica Monolithic Column for Capillary Electrochromatography 混合模式硅胶基质毛细管电色谱整体柱的制备及其电色谱性能研究
- Preparation of Weak Anion-Exchange Silica Monolithic Column for Capillary Electrochromatography 弱阴离子交换硅胶整体柱的制备及其电色谱性能
- Keywords capillary electrochromatography(CEC);norvancomycin;silica monolithic column;preparation;chiral separation; 毛细管电色谱;去甲万古霉素;硅胶整体柱;制备;手性分离;
- silica monolithic column 硅胶整体柱
- The separation on MIP-derivatized silica monolith was superior to that on the organic monolith. 在分子印迹聚合物衍生硅胶整体柱表现仍然好于分子印迹有机整体柱。
- The separation on MIP-deriatized silica monolith was superior to that on the organic monolith. 在分子印迹聚合物衍生硅胶整体柱表现仍然好于分子印迹有机整体柱。
- Then the MIP coating was copolymerized and anchored onto the surface of the silica monolith. 然后分子印迹化合物通过与硅胶整体柱上的烯基发生共聚反应从而固定在其表面。
- Monolithic column has quickly become a well-established phase form in capillary electrochromatography(CEC). 电色谱整体柱是通过原位聚合或固化于柱管内部的方法来制备的一种新型色谱柱。
- The inyl groups were first introduced onto the silica monolith by immobilization of -methacryloxypropyltrimethoxysilane. 首先通过将3-甲基丙烯基氧丙基化三甲氧基硅烷固定在硅胶整体柱表面引入烯基官能团。
- The molecularly imprinted monolithic column is developed in HPLC,due to its simple preparation,high selectivity and low flow resistance. 分子印迹整体柱具有制备简单、特异选择好及传质阻力低等优点,在高效液相色谱中的应用发展迅速。
- After optimization of separation conditions, baseline separation of several phenol compounds was performed on the monolithic column. 操作条件优化后,利用该柱基线分离了几种酚类化合物。
- A cinchonine imprinted chiral monolithic column was prepared for the separation of the diastereomers of cinchonine and cinchonidine by in situ molecular imprinting technique. 在等度及梯度洗脱条件下,非对映异构体辛可宁与辛可尼丁被完全分离。
- The monolithic column was also used for the separation of goat serum and five oligonucleotides, and the results proved that the monolithic column is suitable for the separation of biopolymers. 通过对山羊血清和低聚核苷酸的分离分析,证明了所制备的整体固定相适合用于生物大分子的分离纯化。
- Generally, they can be classified into two types: organic polymeric and silica-based monolithic columns. 主要包括有机聚合物型和硅基整体柱两种类型。
- Monolithic columns for capillary electrochromatography has been hot due to its advantages of easy preparation without frit, excellent permeability, and high efficiency. 摘要毛细管电色谱整体柱以其制备相对简单,渗透性好,柱效高等优点,成为电色谱领域中的一个研究热点。
- Organic polymer monolithic column 有机聚合物整体柱
- fluorine-containing monolithic column 含氟有机聚合物整体柱
- fluorine-containing polymer-based monolithic column 含氟聚合物整体柱
- Butyl methacrylate monolithic column 甲基丙烯酸丁酯整体柱
- capillary silica-based monolithic column 毛细管硅胶整体柱